ekstrak kental daun sendok

7/25/2019 Ekstrak Kental Daun Sendok

1/16

EKSTRAK KENTAL DAUN SENDOK(ExtractumPlantaginis majorisFolii Spissum)

Disusun Ole!Aprilia E"a #ara ($$%&%$'%)De*i ari +ulianti ($$%&%$'%')K,s Ram-ani ($$%&%$'$'.)/ntan O"ta*iani ($$%&%$'$&)0uamma- tau1i2 ($$%&%$'%')Amalia Tusaripa ($%&%$'%3)

EKSTRAK KENTAL DAUN SENDOK(ExtractumPlantaginis majorisFolii Spissum)


2/16

/-entitas tum4uan

Sistemati"a tum4uan

Di*isi ! 0a,noliop+ta

Kelas ! 0a,noliopsi-a

Ana" "elas ! Asteri-ae5an,sa ! 6lanta,inales

Su"u ! 6lanta,inaceae

0ar,a ! 6lanta,o

7enis !Plantago major L8Nama in-onesia ! -aun sen-o"


3/16

0or1ol,i -aun sen-o"

Terna taunan9 tin,,i .:;% cm8 Daunn+a tersusun -alamroset a"ar9 4entu" 4un-ar telur sampai lanset mele4ar9pin,,ir atau 4er,eri,i "asar ti-a" teratur9 pan


4/16

6emerian simplisia

$8 Or,anolepti".>arna ! i


5/16

38 0i"so"opi". Epi-ermis atas ! Ter-iri -ari sel 4esar +an, terentan, tan,ensial9 4entu"

poli,onal -en,an -in-in, sampai lurus atau 4er-in-in, a,a" men,,elom4an,9"uti"ula


6/16

6enampan, melintan, -aun sen-o"

Keteran,an ,am4ar !$8 Ram4ut "elen


7/16

Te"nolo,i e"stra"si

0eto-e pem4uatan e"stra" !

E"stra" -i4uat -en,an cara maserasi men,,una"an etanol'8 Satu 4a,ian ser4u" "erin, -aun sen-o" -imasu""an "e-alam maserator9 -itam4a $% 4a,ian etanol ' -iren-am

selama .


8/16

6emerian e"stra"

5entu" ! "ental

>arna! co"lat tua

5au ! "as

Rasa ! a,a" "elat


9/16

Kan-un,an "imia

Sen+a=a 1la*onoi- antara lain 4ai"alein9 4ai"alin9 api,enin9s"utllarein9 omoplanta,inin9 nepritin9 ispi-ulin9planta,osi-a9 sen+a=a iri-oi- antara lain au"u4in9 39&:-ii-roau"u4in9 .B:O:C( ):,lu"osilau"o4in9 "atalpol9

plantarenalosi-a9 au"u4osi-a9 melitosi-a @ sen+a=aal"aloi- antara lain 4os"ianin9 asam 4os"ia"inat merilester9 tanin9 resin9 saponin9 steroi-9 tio,lu"osi-a8


10/16

0ETODE DAN AS/L 6ENETA6AN 5/LANGAN 6ARA0ETER

$8 6arameter non spesi1i". Ka-ar air ! ti-a" le4i -ari ;9

. Ka-ar a4u total ! ti-a" le4i -ari %9&

. Ka-ar a4u ti-a" larut asam! ti-a" le4i -ari %9&

8 6arameter spesi1i" Sen+a=a i-entitas -an stru"tur "imia

Sen+a=a i-entitas ! 5ai"alein

Stru"tur "imia !


11/16

Kan-un,an "imia -alam e"stra"

$8 6ola "romato,ram

Kromato,ra1i Lapis Tipis (KLT)

Fase -iam ! sili"a ,el GF'& Fase ,era" ! 4utanol:asam asetat ,lasial:a2ua-es (3!$!$)

Dete"si ! perea"si sitr4orat:sinar UH 3.. nm #at pem4an-in, ! rutin

Konsentrasi e"stra" ! '

Holume penotolan ! % Il

7ara" ram4at! ; cm


12/16

Keteran,an !

A ! e"stra" -aun sen-o"5 ! pem4an-in, rutin

Rx ! $8 ; 8 $%% 38 $$; &8 $33 '8 $.%


13/16

8 Ka-ar ,olon,an "an-un,an "imia -an meto-e penetapan

6enetapan "a-ar 1la*onoi- ! 6erea"si

Larutan 0T ! larutan e"sametilentetramin %9' 4J*Larutan l ! larutan asam "lori-a '

Larutan AAG ! larutan asam asetat ,lasial ' *J* -alam metanol

Larutan All3 ! larutan aluminium "lori-a -alam larutan asam asetat

Glasial

Larutan in-u"E"stra" +an, setara -en,an %% m, simplisia -imasu""an "e -alam la4u alas

4ulat9 -itam4a -en,a $ mL larutan 0T9 % mL aseton -an mL larutan l9-ii-rolisis -en,an cara -ire1lu"s selama 3% menit8 ampuran -isarin,men,,una"an "apas9 1iltrat -imasu""an "e -alam la4u teru"ur $%% mL8 Resi-u-ire1lu"s "em4ali -en,an % mL aseton selama 3% menit9 -isarin, -an 1iltrat

-icampur "e -alam la4u teru"ur $%% mL9 campuran 1iltrat -alam la4u teru"ur-itam4a -en,an aseton $%% mL8 Diam4il % mL 1iltrat -imasu""an "e -alamcoron, pisa9 -itam4a % mL air -an -ie"stra"si 3 "ali masin,:masin, -en,an$' mL etil asetat8 Fra"si etil asetat -i"umpul"an -an -itam4a -en,an etil asetatsampai '% mL -alam la4u teru"ur


14/16

Larutan 4lan"o

Diam4il $% mL larutan in-u"9 -itam4a -en,an larutan asam asetat ,lasialsampai ' mL -alam la4u teru"ur8

Larutan sampel

Diam4il $% mL larutan in-u"9 -itam4a -en,an $ mL larutan All3-an larutanasam asetat ,lasial sampai ' mL -alam la4u teru"ur8

6en,u"uran

6en,u"uran -ila"u"an 3% menit setela penam4aan All3 men,,una"an

spe"tro1otometer pa-a pan


15/16

Ke,unaan

$8 6en,,unaan -i-u"un, asil penelitian

Antio"si-an 8

8 6en,,unaan secara tra-isional

Secara tra-isional -i,una"an untu" melancar"an 4uan,air "ecil -an menam4a na1su ma"an8


16/16

ekstrak kental daun sendok

Documents