sakarin fix
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LAPORAN RESMI PRAKTIKUM
KIMIA MAKANAN DAN MINUMAN
“PENETAPAN KASAR SAKARIN”
DIII ANAFARMA
TINGKAT II TAHUN 2013
PROGRAM STUDI D-III ANALIS FARMASI DAN MAKANAN
(ANAFARMA)FAKULTAS FARMASI
LABORATORIUM KIMIA ANALIS AIR, MAKANAN DAN MINUMANINSTITUT ILMU KESEHATAN (IIK)
BHAKTI WIYATA KEDIRI201!201"
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BAB I
PENDAHULUAN
1.1 Latar Belakang
S#$%$&' #&'& *#&$&'+& .#%/*/& $&/%$
*+&& & *$&/*& $I&&#$, #4 #%5$ .#&$&'+&
.%/+$ *$&/*& %$&'& &' #%#% $*%+6 P
*$&/*& %$&'& #%$&' $*+& .#&'7# & .#*&$
/& &' +%& .#%4/ $.#%$+&, +%#& .$4
+&/*$& #%4#$& . *#*+& +##&
(89&, 2000)6
P#*+$& & .#&'7# %$ / $$ *#&'/&/&'+&
+%#& #&'& & .#&'7#, & .&'& .
$#+& %$ +#$/.& *$+%6 B$+ &' #%$: .'#&
&' . *#&#+& +#%9/&& / '&''/& +##&
4$&& */./& *$+%$4 &' &&.'#& &' *#&#+&
+#%/+& & .&'&, *$4& .#*//+&6 N*/& $ $$
4$&, & .#&'7# . %& 4 #&7 +$*$ &'
*#%/.+& & $&' &' */+ #%* & .&'&
&' $+&/*$6 A.$4 *9* .#*+$& & .&'& &
$& $+ $/% & $7$, +#*/&'+$&& #%
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4&'/&' / +*/4$: *$4& .$4 & .#&'7# &'
$'/&+& #%$: +%$&'#&$+6 D4* +#$/.& *#%&
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#.#%$ #+%&' $&$ &+ $5/*.$ .#*+$& &
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*#*.#%&+& +/4$& & *#*$4$+$ /*/% $*.& 4#$
4* #$&'' *#*.#%4/ 5&'+/& $%$/$& ( W$&/,
200< )6
P#*&$ *#%/.+& #&7 +$*$ &' #%$&'
$*+& & $'/&+& /&/+ .%/+ 4& .&'&,$&/%$, #% *$&/*& & *+&& +##&6 P#*&$
#%:/&'$ /&/+ *#&$&'++& 9$ % & %*, *#*.#%$+$
$:-$: =$+, #'$ .#&'7#, *#*.#%$+$ $:-$: +$*$
#+4$'/ *#%/.+& /*#% +4%$ &' .#&$&' '$ //,
*#&'#*&'+& 5#&$ *$&/*& & *+&& #&'& 5/*4
&' #%+&%4, *#&'&%4 .%'%* .#*#4$%& &
.#&/%/&& #% &, *#&'/%&'$ +#%/+& '$'$, & #'$
& /$/$ .#*&$ /*6 P#%+#*&'& $&/%$ .&'&
& *$&/*& +& +#//& .#*&$ %$ /& +#/&
#*+$& *#&$&'+6 I&/%$ .&'& & *$&/*& 4#$
*#&/+$ *#&''/&& .#*&$ $&#$ +%#& %'& %#4$:
*/%, $&'+ +#*&$& .#*&$ $&#$ 5/ 4#$ $&''$ %$
.#*&$ 4*$6 H4 #%#/ *#&'+$+& #%/ *#&$&'+&
.#&''/&& .#*&$ $&#$ #%/* +%$& & $+4*6
M#&/%/ U&&'-/&&' RI N6> T/& 1??< #&&'
.&'&, . II *#&'#&$ +#*&& .&'&6 P4 10
#&&' B& T*& M+&& $9&/*+&, (1) “ S#$.
%&' &' *#*.%/+$ .&'& /&/+ $#%+& $4%&'
*#&''/&+& & ../& #'$ & *& .&'&
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&' $&+& #%4%&' / *#4*./$ *&'
*+$*4 &' #4 $#.+&6 (2) “P#*#%$& *#&#.+&
4#$ 4&5/ & &' $4%&' & / . $'/&+&
#'$ & *& .&'& & +#'$& / .%#
.%/+$ .&'& #% *&' *+$*4 #'$*&
$*+/ . (1) ( D#.+# RI, 1??@ )6
A.$4 *9* .#*+$& & .&'& & $&
$+ $/% & $7$, +#*/&'+$&& #% *#&$*/4+&
+#%/'$& '$ .#*+$&, $+ &' #%$: 4&'/&' *$4&
+#%9/&& /./& &' $+ #%$: 4&'/&' / +*/4$: *$4& .$4 & .#&'7# &' $'/&+& #%$:
+%$&'#&$+6
1.2 Tujuan
T/5/& 4* .%+$+/* .#&#.& +% +%$& 4
U&/+ *#&'#/$ +% +%$& 4* *.#46
1.3 Met!e
M## &' $'/&+& /&/+ .%+$+/* .#&#.& +%
+%$& 4 *## 4+4$*#%$6
1." Pr#n$#%
S+%$& $*+& #&'& H4 +#*/$& $ #+%$
#&'& ##% $ /.+& #&'& *#&#*+& #& &#%46
R#$/ $ $%$ #&'& NOH 060"N6
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<
BAB II
TIN&AUAN BAHAN
2.1 Da$ar Ter#
P#*&$ *#%/.+& #&7 *$*$ &' #%$&'
$*+& & $'/&+& /&/+ .%/+ 4& .&'&,
$&/%$ #% *$&/*& & *+&& +##&6 P#*&$
#%:/&'$ /&/+ *#&$&'++& % & %*, & *#*.#%$+$
$:-$: +$*$ #+4$'/ *#%/.+& /*#% +4%$ &' .#&$&'
'$ //, *#&'#*&'+& 5#&$ *$&/*& & *+&&
#&'& 5/*4 &' #%+&%4, *#&'&%4 .%'%*
.#*#4$%& & .#&/%/&& #% &, *#&'/%&'$
+#%/+& '$'$, & #'$ & /$/$ .#*&$ /*6
P#%+#*&'& $&/%$ .&'& & *$&/*& +& +#//&
.#*&$ %$ /& +#/& #*+$& *#&$&'+6 I&/%$ .&'&
& *$&/*& 4#$ *#&/+$ *#&''/&+& .#*&$ $&#$
+%#& %'& %#4$: */%, $&'+ +#*&$& .#*&$
$&#$ 5/ 4#$ $&''$ %$ .#*&$ 4*$6 H4 #%#/
*#&'+$+& #%/ *#&$&'+& .#&''/&& .#*&$
$&#$ #%/* +%$& & $+4* (W$&/, 200<)6
.#*&$ $&#$ *#%/.+& C &' .
*#&$*/4+& % *&$ / . *#*&/ *#*.#%5*
.#&#%$*& #%. % *&$ #%#/, #&'+& +4%$
&' $$4+&& 5/ 4#$ %#& %$. '/4 (W$&%&,
1??>)6
S+%$& $#*/+& #&'& $+ #&'5 4# F#4%' &
R#*#& . /& 1@?>6 K#$+ .#%* $#*/+& +%$&
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>
$'/&+& #'$ &$#.$+ & .#&'7#, #.$ #5+ /&
1?00 $'/&+& #'$ .#*&$6 S+%$& #&'& %/*/
>H"NO3S & #% *4#+/4 1@3,1@ #9% 4/ $'/&+&
#'$ .#&''&$ '/4 +%#& *#*./&$ $: &' $4,
&&+%$&'#&$+, &$4$ +4%$ %#&, & %'& %#4$: */%,
#4$& $/ +%$& &+ $'/&+& /&/+ *#&'$ /+%
'$ .#&#%$ $## *#44$/ / /&/+ & .&'& &'
#%+4%$ %#& ($, 200<)6
S#'$ .#*&$ +%$& $& #%#&/+ '%*
+4$/*, +4$/*, & &%$/* +%$& #&'& %/*/ +$*$(1H@N2O<S263H2O), (>HKNO3S62H2O), (>HNNO3S62H2O)6
S#9% /*/* '%* +%$& #%#&/+ +%$4 ./$, $+
#%/ / #%/ %*$+ 4#*, & */ 4%/ 4* $%,
#% #% *&$6 S+%$& *#*$4$+$ $&'+ +#*&$& %#4$:
##% 300 *.$ #&'& "00 +4$ $&'+ +#*&$& /+%
#&'& &. &$4$ +4%$6 K*$&$ .#&''/&&& #&'&
.#*&$ 4$&& #%$: $&#%'$ I&#&$ &%$/* +%$&
9/+/. $&''$ $/ 200->00 +4$ /+% 106 $*.$&' %
*&$, +%$& 5/' *#*./&$ % .$ &' $#+& 4#
.#*/%&$& &' %#& %$ .%# $&#$+6 P#*#%$&
I&&#$ *#&'#4/%+& .#%/%& *#44/$ M#&#%$ K##& RI
N620@!M#&+#!P#%!I!1?@" /&/+ .#*&$ /& &
N6>22!M#&+#!P#%!I!1?@@ #&&' B& T*& P&'&,
7 . .&'& & *$&/*& 4& +// $/ #%+4%$
%#& & /&/+ .#&#%$ .#&+$ D$## *#44$/ +%
*+$*/* +%$& &' $.#%4#+& 4 300 *'!+'6
D*.+ .#&''/&& &%$/* +%$&, $ 4* //
&%$/* +%$& $+ *#&'4*$ *#4$*# #$&''
$#++%#$+& 4* /%$&# &. .#%/& +$*$6 B##%.
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@
.#$$& *#&'#&$ *.+ +&/*$ +%$& #%. //
*&/$ *$ *#&/&5/++& $4 &' +&;#&$&46 H$4
.#$$& N$&4 A9#* : S9$#&9# /& 1?<@ *#&+&
7 +&/*$ +%$& 4# %&' #7 #&+ 1 '%*
/ 4#$ *#&#+& #%5$& '&''/& +##&6 P
.#$$& 4$& *#&#/+& +%$& . $ &' $&''$
. *#&#+& +&+#% . #7& .#%9&6 P /&
1?>> & H#4 P%#9$& B%&9 *#4.%+& 7
+%$& #%&''/&' 57 #%5$& +&+#% +&/&' +#*$6
S#5+ $/ $4%&' .#&''/&& +%$& $ & (W$&/,
200<)6
P%+$+/* $&$ *#&''/&+& *## 4+4$*#%$6 T$%$
4 .%# .#&#&/& &+& // 4%/& #&'&
+&#&%$ &' $+#/$ & $.#%4/+& /&/+ #%#+$ #9%
4#&'+. & #5/*4 9& #%#&/ &' +& $&4$$6
P%#/% &4$$ &' *#4$+& $%$ #&'& 4%/& - 4%/&
&' +&#&%$& $+#/$ $#/ &4$$ ;4/*#%$6 D4*
&4$$ 4%/& * & , $%$ *#4$+& .#&'/+/%&
&' #+*, ;4/*# ;4/*# // * & //
&' .4$&' #. 4$&' *#&#%4+&6 4+4$*#%$ $/
*#&''/&+& $%& 4%/& &% /&/+ *#&#&/+&
*6
2.2 T#njauan Ba'an
16 AQUADEST (F III, hal 98)
Nama Resmi : AQUA DESTILATE
Nama Lain : Air Suling
RM!M : "#$ %8,&#g
mol
'elaruan : Laruan alam ean*l gliser
+emerian : airan -ernih, ia. /er0arna, ia. /er/au, ia. /erasa
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'egunaan : Se/agai +elaru
+en1im2anan : em2a eruu2 ra2a
#3 NATRIUN "IDR$'SIDA (F III, hal 9%#)
Nama Resmi : NATRII "4DR$54DUM
Nama Lain : Narium "ir*.sia
RM!M : Na$" 6&,&&g
mol
'elaruan : sanga muah laru alam air an ean*l (97)
+emerian : /enu. /aang, /uiran masaha/lur aau .e2ing, .ering
ra2uh an muah meleleh /asah saanga al.alis an
.*r*si
'egunaan : se/agai a am/ahan
+en1im2anan : alam 0aah eruu2 ra2a /ai.
;3 ASAM 'L$RIDA (F III, hal <69) Nama Resmi : AIDUM "4DR$"L$RIDUM
Nama Lain : asam .l*ria
RM!M : "I ;<,6<g
mol
'elaruan : Laruan alam ean*l, asam asila an air
+emerian : airan ia. /er0arna, /erasa2, /er/au merangsang -i.a
ien=er.an asa2 an /au hilang
'egunaan : se/agai a am/ahan
+en1im2anan : alam 0aah eruu2 /ai.
63 ASAM $'SALAT
Nama Resmi : AIDUM $5ALIUM
Nama Lain : Asam $>ala
RM!M : "##$6 %#<,&?g
mol
'elaruan : Laruan alam air an ean*l 2e.a 9<
+emerian : ser/u. ha/lur, ia. /er0arna
'egunaan : Se/agai a am/ahan
+en1im2anan : alam 0aah eruu2 /ai.3
73 ASET$N (FI I@, hal #?)
Nama Resmi : AET$NUM
Nama Lain : Ase*n
RM!M : ";$"; 78,&8g
mol
'elaruan : a2a /er=am2ur engan air ean*l an .l*r**rm
+emerian : airan ras2aran, ia. /er0arna, /er/au .has, muah
mengua2
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+en1im2anan : alam 0aah eruu2 ra2a /ai.3
<3 DIETIL ETEL
Nama Resmi : DIETI ETER
Nama Lain : Dieir Eer
RM!M : #"7 $'elaruan : Laruan alam %& /ag air, laruan alam ean*l 97 an
.l*r**rm +
+emerian : Laruan ia. /er0arna, muah mengua2, sanga muah
er/a.ar
+en1im2anan : alam 0aah eruu2 /ai.
?3 INDI'AT$R ++ (FI I@, <<#)
Nama Resmi : +"EN$L+ TALEINUM
Nama Lain : Fen*l2 Talein
RM!M : # $"%6 &g ;%8,;; gm*l
'elaruan : 2ra.is, ia. laru alam air laru alam ean*l, aga.
su.ar laru alam .r*l**rm
+emerian : ser/u. ha/lur, 2uih aau 2uih .e.uningan, ia. /er/au
'egunaan : Se/agai ini=a*r
+en1im2anan : alam 0aah eruu2 /ai.
83 !T!
Nama Resmi : AQUA DESTILATE
Nama Lain : !iru !i*im*
'elaruan : 2raliis ia. laru alam air laru alam ean*l (97) +
+emerian : ser/u. .emerahan,
'egunaan : Se/agai Ini.a*r +en1im2anan : alam 0aah eruu2 /ai.
2.3 Reak$#1) R#+$ &%$$ NOH #&'& H22O
H22O 2 NOH N22O 2 H2O
2) R#+$ .#&#.& +% +%$&
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BAB III
METODOLOGI
3.1 Alat
Ala 1ang iguna.an 2aa +enea2an 'aar Sa.arin ianaran1a La/u
erlenme1er #7& ml, /ea.er glass #7& ml, gelas u.ur #7 ml, 2i2e *lume %& ml,
/ure #7 ml, 2i2e ees, =*r*ng 2isah, .a.i iga, lam2u s2irius, .*re. a2i, as/es3
3.2 Bahan
!ahan 1ang iguna.an 2aa +enea2an 'aar Sa.arin ianaran1a !a.u
2rimer "##$6 &,&7 N3 !a.u se.uner Na$" &,&7 N3 Laruan ieil eer, Laruan
Ase*n 7& 3 Laruan "l 2e.a, ini.a*r ++ %, ini.a*r !i! % , sam2el
sa.arin3
3.3 Prosedur
a) Sanarisasi Na$" engan "##$6
"##$6
B Dimasu..an %&,& ml "##$6 &,&7 N
B Dimasu..an la/u erlenme1er #7& ml
B Diam/ah.an ini.a*r ++ % se/an1a. ; ees
BDiirasi engan Na$" sam2ai er-ai 2eru/ahan 0arna men-ai merah
mua3
"ASIL
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/) +enea2an 'aar Sa.arin
"ASIL
Sam2el
- Di2i2e #7,& ml sam2el, .emuian imasu..an .ealam =*r*ng 2isah3
- Diam/ah.an %& ml "l 2e.a, .emuian
- Diam/ah.an %& ml ieil eer
- Dila.u.an e.sra.si se/an1a. ; .ali
- Di.um2ul.an ra.si eer an i=u=i engan %& ml aCuaes se/an1a. ;
.ali
- Diua2.an ra.si eer iaas 2enangas engan haiBhai3 "ingga .iraB.ira 7
ml iang.a an i/iar.an sisa eer mengua2
- Dilaru.an resiu alam 7 ml laruan ase*n 7& iam/ah.an 7 ml "#$
- Diam/ah.an ini.a*r !T! % se/an1a. ; ees
- Diirasi engan Na$" sam2ai er-ai 2eru/ahan 0arna men-ai /iru
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BAB IV
HASIL DAN PEMBAHASAN
.1 Data has!l Pen"a#atan
63%3% Sanarisasi Na$" engan "##$6
N*3 +erla.uan +engamaan
%3 Di2i2e %&,& ml "##$6 &,&7N3
Dimasu..an .ealam la/u erlenme1er
#7& ml
Laruan "##$6 &,&7 N /er0arna -ernih
#3 Diam/ah.an ini.a*r ++ % se/an1a.
; ees
Laruan ini.a*r ++ % /er0arna
-ernih
Laruan =am2uran /er0arna -ernih
;3 Diirasi engan Na$" &,&7 N sam2ai
/eru/ah 0arna men-ai merah mua
Laruan "##$6 &,&7 N /er0arna
-ernih
Laruan hasil irasi /er0arna merah
mua .*nsan3
63%3# +enea2an 'aar Sa.arin
N*3 +erla.uan +engamaan
%3 Di2i2e #7, & ml sam2el .emuian
imasu..an =*r*ng 2isah
Sam2el /er/enu. laruan /er0arna
-ernih
#3 Diam/ah.an %& ml "l 2e.a, an
iam/ah.an %& ml ieil eer
Laruan "l 2e.a /er0arna -ernih
Laruan ieil eer /er0arna -ernih
Laruan =am2uran /er0arna -ernih
;3 Die.sra.si se/an1a. ; .ali63 Di.um2ul.an ra.si eer an i=u=i
engan %& ml aCuaes se/an1a. # .ali
Laruan aCuaes /er0arna -ernih
73 Diua2.an ra.si eer hingga .iraB.ira 7
ml
Diua2.an an i/iar.an sam2ai sisa
eer mengua2
<3 Dilaru.an resiu alam 7 ml ase*n 7&
an iam/ah.an 7 ml "#$
Laruan ase*n 7& /er0arna -ernih
Laruan "#$ /er0arna -ernih
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Laruan =am2uran /er0arna -ernih
?3 Diam/ah.an ini.a*r !T! %
se/an1a. ; ees
Laruan !T! % /er0arna .uning
Laruan =am2uran /er0arna .uning
mua83 Diirasi engan Na$" sam2ai er-ai
2eru/ahan 0arna men-ai /iru
Laruan Na$" /er0arna -ernih
Laruan hasil irasi /er0arna /iru
.2 Data Has!l Per$o%aan
63#3% Sanarisasi Na$" engan "##$6 &,&7 N
N*3 !a.u +rimer @*lume (ml) !a.u Se.uner @*lume (ml)
%3 "##$6 &,&7 N %&,& ml
%&,& ml
Na$" &,&7 N %3 %,?&&
#3 #3 %,?&&
Reraa : %, ?&& ml
63#3# +enea2an 'aar Sa.arin
N*3 Sam2el @*lume (ml) !a.u Se.uner @*lume (ml)
%3 Sa.arin #7,& ml Na$" &,&7 N #;,67&
#3
.3 Perh!tun"an
63;3% Sanarisasi Na$" engan "##$6 &,&7 N
@ > N (Na$") @ > N ("##$6 )
%,?&& > N %& > &,&7
N &,#96% N
63;3# +enea2an .aar sa.arin
'aar sa.arin
(m l x N ) NaOH x BE sakarin x 1000
¿
gram sampel
(23,450 x0,2941 ) x183,18 x1000
41,4
¿30.515,2 ppm
. Pe#%ahasan
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+ra.i.um +enea2an 'aar Sa.arin engan me*e Al.alimeri3 Me*e
Al.alimeri /er2rinsi2 2aa 2eneralan asam /asa3 Me*e ini mengguna.an
Laruan !a.u 2rimer "##$6 &,&7 N an Laruan !a.u Se.uner Na$"3 +aa
2ra.i.um .ali ini mengguna.an ini.a*r ++ % an !T! %3 +ra.i.um ini
mengguna.an ala /ahan anara lain : erlenme1er #7& ml, gelas u.ur, /ure, /ea.er
glass, =*r*ng 2isah, la/u u.ur3 AlaBala se/elum iguna.an unu. 2ra.i.um
harus i/ersih.an ari .**ranB.**ran an i.ali/rasi engan aCuaes3 *r*ng
2isah an /ure harus i/ersih.an le/ih ahulu an i.ali/rasi engan laruan
1ang a.an iguna.an3 *r*ng 2isah iguna.an unu. e.sra.si 1ang memisah.an
anara ua laruan 1ang /erasar.an 2er/eaan .e2*laran3 !ure harus /enarB
/enar /ersih .arena iguna.an unu. sanarisasi an 2enea2an .aar3 Dimana
se/elum iguna.an harus i/ersih.an engan laruan /a.u se.uner, 1aiu Na$"3
+enea2an .aar an sanarisasi ila.u.an engan elii an /enar3
+enea2an .aar sa.arin ila.u.an engan ua aha2an 1aiu sanarisasi
an 2enea2an .aar3 Sanarisasi ila.u.an engan u-uan unu. mengeahui
n*rmalias laruan se.uner3 Sanarisasi 2erama ila.u.an i 2i2e %&,& ml
"##$6 &,&7 N imasu..an ialam erlenme1er #7& ml, iam/ah.an engan
ini.a*r ++ % ; ees3 'emuian iirasi engan Na$" sam2ai 2eru/ahan
0arna men-ai merah mua3
Taha2 .eua 1a.ni 2enea2an .aar sa.arin3 +eramaBama sam2el
imasu..an se/an1a. #7,& ml .ealam =*r*ng 2isah3 *r*ng 2isah ini iguna.an
unu. menge.sra.si ua laruan 1ang /er/ea /erasar.an .e2*larann1a3
'emuian iam/ah.an %& ml "l 2e.a, 2enam/ahan "l ini /eru-uan unu.
mengasam.an sam2el3 Diam/ah.an lagi engan %& ml ieil eer iguna.anunu. menge.sra.si sa.arin3 Laruan erse/u ie.sra.si .ealam =*r*ng 2isah
se/an1a. iga .ali3 E.sra.si ini iguna.an unu. memisah.an 2elaru sehingga
2en1usunB2en1usun erse/u er2isah ari 2elaru lain 1ang ia. laru3 Laruan
1ang iguna.an unu. e.sra.si 1aiu eer3 +aa saa e.sra.si ilea..an iaas
.arena /era -enis le/ih renah an sa.arin erlea. i/a0ah .arena /era -enis
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le/ih /esar3 'emuian i.um2ul.an ra.si eer 1ang ia2a ari e.sra.si,
.emuian i/ilas engan %& ml aCuaes se/an1a. ua .ali 1ang /eru-uan unu.
mem/ilas su2a1a ia. aa e.sra. 1ang eringgal3 Diua2.an .iraB.ira hingga
ersisa 7 ml3 Laruan resiun alam 7ml laruan ase*n 7& i am/ah.an 7ml
"#$3 Diam/ah.an !T! % se/an1a. ; ees an i e.sra.si engan Na$"
sam2ai er-ai 2eru/ahan men-ai 0arna men-ai /iru3 +aa saa e.sra.si harus
haiBhai .arena 1ang i guna.an aalah 2elaru eer 1ang menim/ul.an /au 1ang
men1enga an a2a menim/ula.n rasa nganu., a2a menga.i/a.an gaal -i.a
er.ena angan3 E.sra.si engan =*r*ng 2isah engan mem/u.a an menuu2
.eran 2aa saa e.sra.si3 'ran i /u.a /erun-uan unu. menghilang.an gas,
1ang i im/u.lan 2elaru3 i.a ia. era2a gas a2a i.aa.an e.sra.si elah
/era.hir3 'emuian e.sra. i=am2ur sam2ai h*m*ngen3
"asil 2ra.i.um sanarisasi 1ang ila.u.an ua .ali re2li.asi engan hasil
%,?&& ml ari hasil erse/u a2a i 2er*leh raaBraa %,?&& ml an i 2er*leh
n*rmalias Na$h &,#96% N3 "asil ari 2enea2an .aar i 2er*leh #;,67& ml3
+enea2an .aar sa.arin i a2a.an gram sam2el 6%,6 gram i2er*leh ari /era
-enis m .aar sa.arin i2er*leh hasil ;&37%7,# 22m3 "asil 1ang ia2a.an
i/aning.an engan +ERMEN'ES RI N$3%&?9AS'?9 ahun %9?9 unu.
sa.arin 1ang meme2er/*leh.an 2enggunaan sa.arin alam .aar ma.simun unu.
2eneria ia/ees milius .aar ma.simum sa.arin i 2er/*leh.an aalah 7,%7
22m3 Seang.an 2aa ma.anan aalah &,&&7 22m3 'aar erse/u sanga mele/ihi
2ers1araan halBhal 1ang mem2engaruhi 2em/uaan laruan sanar 1ang salah3
'esalahan 2aa 2ra.i.um 1nag .urang elii alam 2em/a=aan ii. a.hir irasi3
Ala 1ang i guna.an .urang /ersih ari .esalahan ari 2ra.i.um alam
2enam/ahan laruan 1ang .urang sesuai3
'esehaan /agi manusia sanga 2ening /agi manusia *leh .arena iu /an1a.
meng.*nsumsi /ahan 2emanis am/ahan sa.arin engan /erle/ihan a.an
menga.i/a.an 2en1a.i ia/ees, .an.er .an*ng .emih, ins*mia, iare, sa.i
2eru, hi2erensi 1ang sanga merugi.an u/uh3 Men-aga .esehaan sanga 2ening
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meng.*nsumsi gula aau /ahan am/ahan 2emanis ia. /*leh /erle/ihan an
harus sesuai engan .aar 1ang ienu.an3
BAB V
PEN&T&P
'.2 (es!#)ulan
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!erasar.an hasil 2ra.i.um 2enea2an .aar sa.arin alam sa.arin % i
a2a.an .aar sa.arin se/esar ;&37%7,# 22m3
'.3 Saran%3 se/elum 2ra.i.um harus mengeri an memahami a.an 2r*seur
1ang a.an i la.u.an3
#3 0a-i/ mengguna.an A+D (Ala +engaman Diri)
;3 alaBala 1ang iguna.an harus /ersih
63 .urang eliin1a saa 2em/a=aan a.hir irasi
73 .urang eili saa 2enim/angan sam2el an 2emi2ean laruan3
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DA*TA+ P&STA(A
Di-en +$M3 %9?93 Farmakope Indonesia edisi III”. a.ara : De2aremen
'esehaan RI
Di-en +$M3 %9973 Farmakope Indonesia edisi IV”. a.ara : De2aremen
'esehaan RI
Gan-ar, I/nu Gh*li/ an A/ul Rahman3 #&&?3 Kimia Farmasi Analisis”.
4*g1a.ara : 2usa.a 2ela-ar3
"ar-ai, %99;3 Ilmu Analitik Dasar H3 a.ara : Grameia3
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0
LAMPI+AN
+em/uaan reagen:
%3 "##$6 &,&7 N %&& ml
Gram N x
BM
Val x
Vol
1000
0,05 x
126,07
2 x 100
1000
&,;%7% gram
ara 2em/uaan :
B Diim/ang "##$6 se/an1a. &,;%7% gram
B Dimasu..an .ealam /ea.er glass %&& ml
B Diam/ah.an aCuaes ?& ml, .emuian iau. sam2ai laru
B Di2inah.an .ealam la/u u.ur %&&ml, i am/ah.an aCuaes sam2ai ana
/aas, .*=*. hingga h*m*ngen3
#3 Na$" &,&7 N 7&& ml
Gram
N x BM
Val
x Vol
1000
0,05 x
40
1 x 500
1000
% gram
ara 2em/uaan :
B Diim/ang Na$" se/an1a. % gram
B Dimasu..an .ealam /ea.er glass 7&& ml
B Diam/ah.an aCuaes /e/as $# ;&& ml, .emuian iau. sama2i laru
B Di2inah.an .ealam la/u u.ur 7&& ml, iam/ah.an aCuaes /e/as $# sam2ai
ana /aas, Di.*=*. hingga h*m*ngen3
;3 Sa.arin % 7 ml
Gram 1
100 x100ml
% gram
ara 2em/uaan :
B Diim/ang % gram sa.arin, iuang .ealam /ea.er glass %&& ml
B Diam/ah.an aCuaes sam2ai ana /aas, iau. sam2ai ana /aas3
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63 ++ % %&& ml
Gram 1
100 x100ml
% gramara 2em/uaan :
B Diim/ang %g +hen*l +laein, imasu..ann .ealam /ea.er glass
B Diam/ah.an sei.i ean*l, iau. sam2ai h*m*gen3
B Diam/ah.an ean*l sam2ai ana /aas, au. sam2ai laru3
73 !T! % %&& ml
Gram 1
100 x100ml
% gram
ara 2em/uaan :B Diim/ang %g !T!, imasu..ann .ealam /ea.er glass
B Diam/ah.an sei.i ean*l, iau. sam2ai h*m*gen3
B Diam/ah.an ean*l sam2ai ana /aas, au. sam2ai laru3
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